Announcement
Starting on July 4, 2018 the Indonesian Publication Index (IPI) has been acquired by the Ministry of Research Technology and Higher Education (RISTEKDIKTI) called GARUDA Garba Rujukan Digital (http://garuda.ristekdikti.go.id)
For further information email to portalgaruda@gmail.com

Thank you
Logo IPI  
Journal > Journal of Chemistry > STUDI REAKSI SIKLOPENTILSILAN DENGAN 4-IODIDA THIOANISOL MENGGUNAKAN KATALIS PALADIUM

 

Full Text PDF (278 kb)
Journal of Chemistry
Vol. 7, No. 2 Juli 2013
STUDI REAKSI SIKLOPENTILSILAN DENGAN 4-IODIDA THIOANISOL MENGGUNAKAN KATALIS PALADIUM
Article Info   ABSTRACT
Published date:
17 Jul 2013
 
A study on cyclopentylsilane reaction in tetrahydrofuran with 4-iodo thioanisol has been carried out using palladium as catalyst under argon atmosphere at room temperature. The results showed that the product was tris(4-thioanisyl)cyclopentylsilane (1) which was obtained from recrystallization using methanol with the yield 35%. The Compound (1) has a melting point of 91.5-92.0 oC. Analysis using GC-MS found m/z 466 with six equivalent protons and eight carbons peak obtained from 1H and 13C NMR.
Copyrights © 2013